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- W2023505139 abstract "Abstract A protocol for the preparation of novel triblock copolymers comprising a polyrotaxane center block and outer blocks of poly( N -isopropylacrylamide) (PNIPAAm) as bulky stoppers was developed, in which N -isopropylacrylamide was allowed to telomerize in the presence of polypseudorotaxanes made from the self-assembly of thiol end-capped PEG with a varying amount of α-CDs under UV irradiation in aqueous solution. The molecular structure of the resulting copolymers was characterized in detail by 1 H NMR, FTIR, XRD, TG and DSC analyses. It was demonstrated that the PNIPAAm blocks are successfully attached to the two terminals of the polypseudorotaxanes and each block having the minimum 7 NIPAAm units seems long and bulky enough to efficiently impede the dethreading of α-CDs from the PEG axle to give rise to the triblock polyrotaxane-containing copolymers." @default.
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- W2023505139 date "2006-08-01" @default.
- W2023505139 modified "2023-09-28" @default.
- W2023505139 title "Novel triblock copolymers synthesized via radical telomerization of N-isopropylacrylamide in the presence of polypseudorotaxanes made from thiolated PEG and α-CDs" @default.
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- W2023505139 doi "https://doi.org/10.1016/j.polymer.2006.06.048" @default.
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