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• W2023550100 abstract "Reaction of [NEt4]2[ReBr3(CO)3] with 2,4-pentanedione (acac) yields a complex of the type fac-Re(acac)(OH2)(CO)3 (1) under aqueous conditions. 1 was further reacted with a monodentate ligand (pyridine) to yield a fac-Re(acac)(pyridine)(CO)3 complex (2). Complex 1 was found to react with primary amines to generate a Schiff base (imine) in aqueous solutions. When a mixed-nitrogen donor bidentate ligand, 2-(2-aminoethyl)pyridine, that has different coordination affinities for fac-Re(acac)(OH2)(CO)3 was utilized, a unique tridentate ligand was formed in situ utilizing a metal-assisted Schiff base formation to yield a complex fac-Re(CO)3(3[(2-phenylethyl)imino]-2-pentanone) (3). Tridentate ligand formation was found to occur only with the Re-coordinated acac ligand. Reactions of acac with fac-Re(CO)3Br(2-(2-aminoethyl)pyridine) (4) or a mixture of [NEt4]2[ReBr3(CO)3], acac, and 2-(2-aminoethyl)pyridine did not yield the formation of complex 3 in water." @default.
• W2023550100 created "2016-06-24" @default.
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• W2023550100 date "2008-02-26" @default.
• W2023550100 modified "2023-10-14" @default.
• W2023550100 title "Metal-Assisted In Situ Formation of a Tridentate Acetylacetone Ligand for Complexation of <i>fac</i>-Re(CO)₃⁺ for Radiopharmaceutical Applications" @default.
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• W2023550100 doi "https://doi.org/10.1021/ic701996e" @default.
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