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- W2023561438 abstract "A substrate-controlled stereoselective epoxidation of free and monoprotected homoallylic diols was developed. This second-generation approach is based on the incorporation of a primary hydroxy directing group at the C2 methyl carbon, which changes the nature of the vanadium ester intermediate providing a new diastereoselectivity manifold for the preparation of 3,4-epoxy alcohols. This modification favored the formation of the challenging C2-syn epoxy alcohol product not previously available using the standard homoallylic alcohol substrates. These new epoxy alcohol diastereomers expand the scope and generality for the utilization of 3,4-epoxy alcohols as precursors for stereoselective polypropionate synthesis." @default.
- W2023561438 created "2016-06-24" @default.
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- W2023561438 date "2011-02-01" @default.
- W2023561438 modified "2023-10-17" @default.
- W2023561438 title "Stereoselective VO(acac)2 catalyzed epoxidation of acyclic homoallylic diols. Complementary preparation of C2-syn-3,4-epoxy alcohols" @default.
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- W2023561438 doi "https://doi.org/10.1016/j.tet.2010.11.079" @default.
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