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- W2023577558 abstract "Abstract (1 S ,2 R ,3 S )-, (1 R ,2 R ,3 S )- and (1 S ,2 R ,3 R )-4-amino-1,2,3-trihydroxybutylphosphonic acids were synthesised. The synthetic strategy involved preparation of the respective 4-azido-2,3- O -isopropylidene- l -threose or - d -erythrose, addition of dialkyl phosphites, separation of C-1 epimeric O , O -dibenzyl phosphonates, the reduction of azides and the removal of the protecting groups. The (2 R ,3 S ) and (2 R ,3 R ) configurations in the final products were secured by employing diethyl l -tartrate and d -isoascorbic acid as starting materials. The stereochemical course of the addition to the carbonyl groups in 4-azido-2,3- O -isopropylidene- l -threose or - d -erythrose followed that established earlier for 2,3- O -isopropylidene- d -glyceraldehyde and similar (3:1–4:1) diastereoselectivities were achieved." @default.
- W2023577558 created "2016-06-24" @default.
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- W2023577558 date "2005-12-01" @default.
- W2023577558 modified "2023-09-27" @default.
- W2023577558 title "Enantiomerically pure 4-amino-1,2,3-trihydroxybutylphosphonic acids" @default.
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- W2023577558 doi "https://doi.org/10.1016/j.tet.2005.09.057" @default.
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