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• W2023580286 abstract "Abstract Heteroarm H‐shaped terpolymers, [(poly( L ‐lactide))(polystyrene)]poly(ethylene oxide)[(polystyrene)(poly( L ‐lactide))], [(PLLA)(PS)]PEO[(PS)(PLLA)], in which PEO acts as a main chain and PS and PLLA as side arms, have been successfully prepared via combination of reversible addition–fragmentation transfer (RAFT) polymerization and ring‐opening polymerization (ROP). The first step is the synthesis of the PEO capped with one terminal dithiobenzoate group and one hydroxyl group at every chain end, [(HOCH 2 )(PhC(S)S)]PEO[(S(S)CPh)(CH 2 OH)] from the reaction of carboxylic acid with ethylene oxide. Then, the RAFT polymerization of styrene (St) was carried out using [(HOCH 2 )(PhC(S)S)]PEO[(S(S)CPh)(CH 2 OH)] as RAFT agent and AIBN as initiator, and the triblock copolymer, [(HOCH 2 )(PS)]PEO[(PS)(CH 2 OH)], was formed. Finally, the heteroarm H‐shaped terpolymers, [(PLLA)(PS)]PEO[(PS)(PLLA)], were produced by ROP of LLA, using triblock copolymer, [(HOCH 2 )(PS)]PEO[(PS)(CH 2 OH)], as macroinitiator and Sn(Oct) 2 as catalyst. The target products and intermediates were characterized by 1 H NMR spectroscopy and gel permeation chromatography. © 2007 Wiley Periodicals, Inc. J Polym Sci Part A: Polym Chem 45: 789–799, 2007" @default.
• W2023580286 created "2016-06-24" @default.
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• W2023580286 date "2007-01-08" @default.
• W2023580286 modified "2023-10-17" @default.
• W2023580286 title "Preparation and characterization of heteroarm H-shaped terpolymers by combination of reversible addition-fragmentation transfer polymerization and ring-opening polymerization" @default.
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• W2023580286 doi "https://doi.org/10.1002/pola.21907" @default.
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