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- W2023623082 abstract "Abstract The Ni – B system is reassessed based on critical literature review and the results of key experiments and first-principles calculation. Eight Ni – B alloys are prepared by arc melting the pure elements. The samples are analyzed by means of chemical analysis, X-ray diffraction and differential thermal analysis. NiB 12 and NiB 2 are not found in the equilibrium condition. Four invariant temperatures are measured: 1098 ± 2 °C for L ↔ fcc(Ni) + Ni 3 B, 1114 ± 2 °C for L ↔ Ni 3 B + Ni 2 B, 1025 ± 2 °C for L ↔ Ni 2 B + orthorhombic-Ni 4 B 3 and 1044 ± 2 °C for L + βB ↔ NiB. The heat capacity of NiB is determined to be 58.46092 + 0.0012 · T – 1 597 915.59793 · T – 2 (J mol – 1 K – 1 , T in Kelvin) in the temperature range from 40 to 950 °C by differential scanning calorimetry. First-principles calculation indicates that the energy of inserting a B atom into the interstitial site of the lattice for Ni atoms is lower than that of substituting for an Ni atom with a B atom. Consequently, the sublattice model (Ni) (B, Va) in which B atoms occupy the interstitial sites is employed for the fcc(Ni) phase rather than the model (Ni, B) (Va) in which B atoms substitute for Ni atoms. In addition, the enthalpies of formation for the five compounds are obtained via first-principles calculation to supplement the modeling. A self-consistent set of thermodynamic parameters for the Ni – B system is finally obtained and the calculated results show good agreement with the experimental data." @default.
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- W2023623082 date "2009-01-01" @default.
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- W2023623082 title "Reassessment of the Ni–B system supported by key experiments and first-principles calculation" @default.
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- W2023623082 doi "https://doi.org/10.3139/146.101786" @default.
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