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- W2023644316 abstract "Eine Reihe neuer, pseudooktaedrischer Eisen(III)-Gemischtligandenkomplexe mit Oxalat bzw. Malonat und den aromatischen α-Diiminen 1, 10-Phenanthrolin und 2, 2′-Bi-pyridyl wurde dargestellt. Die Bildung dieser Verbindungen erfolgte sowohl über die protolytische Spaltung der sauerstoffverbrückten Eisen(III)-Zweikernspezies [Fe2(N,N4O)]4+ mit N, N = α-Diimin, als auch durch sukzessive Umsetzung des Eisen(III)-Ions mit den Sauerstoffdonorliganden und anschließender Reaktion mit dem Diimin. In Abhängigkeit vom pH-Wert und dem stöchiometrischen Verhältnis der Reaktionspartner ergeben sich unterschiedliche Komplextypen. Die Charakterisierung der dargestellten lichtempfindlichen Eisen(III)-Verbindungen erfolgte mittels IR, UV/VIS-Spektroskopie, Leitfähigkeitsmessungen sowie magnetochemisch. Oxalate and Malonate Complexes of Iron(III) with Aromatic α-Diimine Ligands A new series of pseudooctahedral iron(III) mixed ligand complexes with oxalate/malonate and aromatic α-diimines 1, 10-phenanthroline and 2, 2′-bipyridine has been prepared. The formation of these compounds proceeds either by acid dissociation of binuclear oxygen bridged complexes of iron(III) [Fe2(N,N4O)]4+ with N,N = α-diimine or by stepwise reaction of iron(III) ions with oxalate/malonate and diimine ligand. In the dependence of pH and stoichiometric conditions different types of photosensitive coordination compounds were obtained which have been characterized by means of IR, UV/VIS spectroscopy, molar conductivity, and magnetic susceptibility measurements." @default.
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- W2023644316 date "1980-09-01" @default.
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- W2023644316 title "Oxalat- und Malonatkomplexe des Eisen(III) mit aromatischen ?-Diiminliganden" @default.
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- W2023644316 doi "https://doi.org/10.1002/zaac.19804680127" @default.
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