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• W2023668703 endingPage "7847" @default.
• W2023668703 startingPage "7842" @default.
• W2023668703 abstract "Metal–organic frameworks (MOFs), a novel class of hybrid inorganic–organic materials, possess high surface area, good thermal stability and selectivity, and thus have great potential for use as sorbent materials. MOF-177 is attractive for its large pores, high adsorptivity and selectivity, which has rarely been used in analytical science. Herein a facile magnetization of MOF-177 for rapid magnetic solid phase extraction of phenols from environmental water samples was studied, with analysis using gas chromatography-mass spectrometry. The magnetization of MOF-177 microcrystals as well as solid-phase extraction (SPE) of phenols was achieved simultaneously by mixing MOF-177 and Fe3O4@SiO2 microparticles in the water sample under sonication. Under the optimized conditions, the developed method showed good linearity within the range of 1–200 μg L−1, low detection limits (16.8–208.3 ng L−1) and quantitation limits (56.0–694.2 ng L−1). The recoveries are between 83.3 and 108.7% with the spiked level of 25 μg L−1. The results demonstrated that the Fe3O4@SiO2–MOF-177 magnetic microspheres are promising sorbents in the MSPE field in environmental samples." @default.
• W2023668703 created "2016-06-24" @default.
• W2023668703 creator A5004981804 @default.
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• W2023668703 date "2014-07-04" @default.
• W2023668703 modified "2023-10-16" @default.
• W2023668703 title "Evaluation of Fe₃O₄@SiO₂–MOF-177 as an advantageous adsorbent for magnetic solid-phase extraction of phenols in environmental water samples" @default.
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• W2023668703 doi "https://doi.org/10.1039/c4ay00822g" @default.
• W2023668703 hasPublicationYear "2014" @default.
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