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- W2023669377 abstract "Abstract In this study, the preparation of novel metal-free phthalocyanine 2, metallophthalocyanine complexes 3, 4, 5, 6 (MPcs, M = Ni, Co, Cu, Fe) with 6-oxyquinoline functional group and quaternized metallophthalocyanine derivatives 3a, 4a, 6a (MPcs, M = Ni, Co, Fe), was achieved. The reaction of 4-(quinolin-6-yloxy)phthalonitrile 1 in 2-(dimethylamino)ethanol as the solvent, the metal-free phthalocyanine 2 was synthesized. The synthesis of metallophthalocyanines 3–6 derived from 4-(quinolin-6-yloxy)phthalonitrile 1 were carried out by microwave irradiation. Aggregation properties of Pcs were investigated at different concentrations in chloroform, dimethylsulfoxide, dimethylformamide and water. The metal-free phthalocyanine 2 showed the aggregation in polar solvent DMSO, whereas in chloroform no aggregation was observed. The effect of the concentration on the aggregation properties of complexes 2, 3, 4 and 5 were studied in chloroform. No aggregation was demonstrated in chloroform from concentration between 1 × 10−5 and 0.4 × 10−5 M. The new compounds have been characterized by using elemental analysis, UV–Vis, IR, 1H NMR, 13C NMR and MS spectroscopic data." @default.
- W2023669377 created "2016-06-24" @default.
- W2023669377 creator A5048631251 @default.
- W2023669377 date "2011-03-01" @default.
- W2023669377 modified "2023-10-09" @default.
- W2023669377 title "Novel water-soluble metal-free and metallophthalocyanines: Synthesis, spectroscopic characterization and aggregation properties" @default.
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- W2023669377 doi "https://doi.org/10.1016/j.synthmet.2010.12.035" @default.
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