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- W2023682808 abstract "Twelve-membered cyclic cis- and trans-β-lactams 1b and 2b and the corresponding cyclic cis- and trans-β-amino acid enantiomers, 1a, 1c and 2a, 2c were prepared through the CAL-B-catalysed enantioselective ring cleavage of racemic cis-13-azabicyclo[10.2.0]tetradecan-14-one, (±)-1, and trans-13-azabicyclo[10.2.0]tetradecan-14-one, (±)-2. High enantioselectivities (E >200) were observed for the ring opening of both the cis- and trans-β-lactams when the Lipolase-catalysed reactions were performed with 0.5 equiv of H2O in i-Pr2O at 70 °C. The resolved β-lactams 1b and 2b (yield ⩾47%) and β-amino acids 1a and 2a (yield ⩾32%) could be easily separated." @default.
- W2023682808 created "2016-06-24" @default.
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- W2023682808 date "2006-12-01" @default.
- W2023682808 modified "2023-10-15" @default.
- W2023682808 title "Do lipases also catalyse the ring cleavage of inactivated cyclic trans-β-lactams?" @default.
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- W2023682808 doi "https://doi.org/10.1016/j.tetasy.2006.11.030" @default.
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