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- W2023704408 abstract "The synthesis of 5′-methyl-2,2′-bipyridine-6-carboxylic acid is described starting from the pivotal 5′-methyl-6-bromo-2,2′-bipyridine building block. Functionalisation of the latest at the 5′-methyl position gives access to the 5′-bromomethyl, 5′-hydroxymethyl and 5′-aminomethyl derivatives. Upon nucleophilic substitution, the hydroxy and amino derivatives react with the 5′-bromomethyl compound to give quasi-linear and podand type intermediates. Thanks to a carboalkoxylation reaction at the 6-bromo position of the different intermediates, followed by a saponification reaction, mono-, bis- and tris-tridentate ligands are obtained, which are particularly well suited for the complexation of lanthanide(III) cations." @default.
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- W2023704408 date "2001-01-01" @default.
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- W2023704408 title "Synthesis of mono-, bis- and tris-tridentate ligands based on 5′-substituted-2,2′-bipyridine-6-carboxylic acid" @default.
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