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• W2023708641 abstract "We report here the use of protonless NMR spectroscopy to extract structural information under biologically relevant conditions when conventional proton-detection NMR spectroscopy fails due to the loss of labile proton resonances. By direct 13C detection, correlations between nonlabile nuclei of a given biomolecule can be determined with high resolution, which becomes particularly useful when the system of interests is sensitive to solvent exchange at elevated temperatures, such as intrinsically disordered proteins. Human α-synuclein, which is associated with Parkinson’s disease, is used as a model system to illustrate the usefulness of protonless NMR spectroscopy in recovering hitherto missing spectral information." @default.
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• W2023708641 date "2009-05-11" @default.
• W2023708641 modified "2023-09-24" @default.
• W2023708641 title "Use of Protonless NMR Spectroscopy To Alleviate the Loss of Information Resulting from Exchange-Broadening" @default.
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• W2023708641 doi "https://doi.org/10.1021/ja902307q" @default.
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