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- W2023709458 abstract "Beta-cyclodextrin is transannularly disulfonylated at the 6(A)- and 6(B)-positions, and then converted to the corresponding 6(A),6(B)-diiodide and 6(A),6(B)-dithiol. Cross-coupling of the latter two species yields a single head-to-head-coupled beta-cyclodextrin dimer 5 with two sulfur linkers at adjacent 6-methylene carbons. NMR and X-ray analysis revealed the trans-type (aversive) linkage of both beta-cyclodextrin units. In the solid-state structure of 5.5 MeOH.23 H(2)O, the undistorted cyclodextrin macrocycles feature almost parallel ring planes pointing away from each other, leaving 5 with a handcuff-like appearance of approximate C(2) symmetry. This work represents the first successful crystallographic study on a cyclodextrin dimer." @default.
- W2023709458 created "2016-06-24" @default.
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- W2023709458 date "2003-07-11" @default.
- W2023709458 modified "2023-10-17" @default.
- W2023709458 title "The First Successful Crystallographic Characterization of a Cyclodextrin Dimer: Efficient Synthesis and Molecular Geometry of a Doubly Sulfur-Bridged β-Cyclodextrin" @default.
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- W2023709458 doi "https://doi.org/10.1002/chem.200204310" @default.
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