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• W2023710100 startingPage "4892" @default.
• W2023710100 abstract "We report a novel comprehensive Fourier transform electrochemical impedance spectroscopic (FTEIS) analysis method of a series of chronoamperometric currents obtained during staircase cyclic voltammetric (SCV) experiments. In our method, FTEIS analysis of a set of chronoamperometric currents recorded upon applying a series of small potential steps during an SCV experiment provides a complete description of an electron-transfer reaction at the electrode/electrolyte interface in forms of equivalent circuit elements. Conversion of the circuit elements thus obtained from the analysis allows electrode kinetic parameters including the electron-transfer rate constant, transfer coefficient, diffusion coefficient, and double layer capacitance as well as thermodynamic parameters such as the half-wave potential and the apparent number of electrons transferred to be determined. Theories for obtaining an ac admittance voltammogram, as well as both the thermodynamic and mass-transfer kinetic parameters thereof, from the SCV data have been developed and verified. A decided advantage of the method is that it provides completely self-contained information regarding an electron-transfer reaction from a single pass of the SCV experiment." @default.
• W2023710100 created "2016-06-24" @default.
• W2023710100 creator A5053285008 @default.
• W2023710100 creator A5071375155 @default.
• W2023710100 date "2007-05-27" @default.
• W2023710100 modified "2023-10-15" @default.
• W2023710100 title "Fourier Transform Analysis of Chronoamperometric Currents Obtained during Staircase Voltammetric Experiments" @default.
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• W2023710100 doi "https://doi.org/10.1021/ac070169w" @default.
• W2023710100 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/17530816" @default.
• W2023710100 hasPublicationYear "2007" @default.
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