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- W2023733223 abstract "Tetrakis(di-tert-butylmethylsilyl)disilene (1) was treated with 2.2 equiv of MNp (metal naphthalenide, M = Na, K) in THF followed by addition of 2 equiv of a crown ether (2b, 15-crown-5; 2c, 18-crown-6), resulting in the formation of the first isolable alkali-metal-substituted silyl radicals 2, which were characterized by both EPR spectra and X-ray crystallography. The lithium-substituted silyl radical 2a was also synthesized as an isolable compound by the reaction of free silylene anion radical with LiBr, and it has a monomeric structure in solution but a dimeric structure in the solid state." @default.
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- W2023733223 date "2008-03-04" @default.
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- W2023733223 title "Isolable Alkali-Metal-Substituted Silyl Radicals (<sup><i>t</i></sup>Bu<sub>2</sub>MeSi)<sub>2</sub>SiM (M = Li, Na, K): Electronically and Sterically Accessible Planar Silyl Radicals" @default.
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- W2023733223 doi "https://doi.org/10.1021/om8000185" @default.
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