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- W2023744569 abstract "Proton noise decoupled 13C NMR spectra were recorded of 23 substituted allenes as neat liqs. at 25.16 MHz. Each Me, Et, and S-alkyl substituent contributed +3.3, +4.8, and +7 g 2 ppm, resp., to the 13Cb chem. shift (d) of R1R2Ca:Cb:CgR3R4. An approx. linear correlation was obsd. between dCb of monosubstituted allenes and dCb of the corresponding monosubstituted vinyl compds. XCaH:CbH2: the slope, .apprx.0.35, indicates that the vinyl C is more sensitive to the substituent effect than is the allenic Cb. For the monosubstituted allenes, dCb decreased approx. linearly with increasing dCg. [on SciFinder (R)]" @default.
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- W2023744569 date "1971-01-01" @default.
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- W2023744569 title "13C NMR spectra of allenes" @default.
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- W2023744569 doi "https://doi.org/10.1016/s0040-4039(01)97163-1" @default.
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