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- W2023800292 abstract "We report the synthesis and characterisation of binuclear η5-pentamethylcyclopentadienylrhenium complexes, [(η5-C5Me5)Re(CO)2]2(μ-E) (E = S (2), Se (3), Te (4)), containing a chalcogen bridge in addition to a ReRe bond. According to the X-ray structural analysis, 3 possesses approximately C2 molecular symmetry; the C5Me5 ring ligands occupy trans positions with respect to the central Re2Se unit [d(ReRe) 3.032(1) Å, ∢ ReSeRe 74.9(1)°]. As expected, the complexes of the now complete series [Cp★Re(CO)2]2(μ-E) (E = O (1), S (2), Se (3), Te (4)) show a high degree of similarity in their corresponding mass, IR, 1H and 13C NMR spectra. Es wird über die Synthese und Charakterisierung zweikerniger η5-Pentamethylcyclopentadienyl-Rhenium-Komplexe [(η5-C5Me5)Re(CO)2]2(μ-E) berichtet, die zusätzlich zu einer ReRe-Bindung eine Chalkogenbrücke (E = S (2), Se (3), Te (4)) enthalten. Nach der Röntgenstrukturanalyse besitzt 3 angenähert die Molekülsymmetrie C2; die C5Me5-Ringliganden nehmen bezüglich der zentralen Re2Se-Einheit" @default.
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- W2023800292 date "1986-01-01" @default.
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- W2023800292 title "Zweikernige η5-pentamethylcyclopentadienyl-rhenium-komplexe mit einer chalkogenbrücke. Die molekülstruktur von [(η5-C5Me5)Re(CO)2]2(μ-Se)" @default.
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- W2023800292 doi "https://doi.org/10.1016/0022-328x(86)82017-4" @default.
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