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- W2023843590 abstract "Radiosynthesis of 2'-deoxy-2'-[(18)F]-fluoro-5-methyl-1-beta-L-arabinofuranosyluracil ([(18)F]-L-FMAU) is reported. Compound 1 was synthesized and converted to 2-triflate 2. Compound 3 was prepared from 2 using tetrabutylammonium[(18)F]fluoride, converted to 4, and then coupled with 5. The crude product was hydrolyzed, and purified by HPLC to obtain 7a. The radiochemical yield of [(18)F]-L-FMAU was 26% decay corrected (d.c.) in four runs with radiochemical purity >99% and specific activity 2200 mCi/micromol. The synthesis time was 3.3-3.5h from the end of bombardment (EOB)." @default.
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- W2023843590 date "2007-08-01" @default.
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- W2023843590 title "Radiosynthesis of 2′-deoxy-2′-[18F]-fluoro-5-methyl-1-β-l-arabinofuranosyluracil ([18F]-l-FMAU) for PET" @default.
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- W2023843590 doi "https://doi.org/10.1016/j.apradiso.2007.04.003" @default.
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