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• W2023854813 startingPage "19639" @default.
• W2023854813 abstract "By using 13C solid-state NMR, monitoring the reactivity of methoxy species with carbon monoxide has been performed on 12-tungstophosphoric acid, H3PW12O40, at 423−473 K. Surface methoxy species have been selectively prepared from methanol at 293−423 K. Almost quantitative conversion of surface methoxy species into acetyl groups bound to the Keggin anion and acetic acid has been observed at 473 K. These data provide unambiguous evidence for the role of methoxy species as the intermediate of methanol and dimethyl ether carbonylation on solid H3PW12O40. The formation of a trimethyloxonium ion has been detected on the surface of heteropolyacid for the first time. The carbonylation of trimethyloxonium proceeds via the analogous mechanism through the methoxy species intermediate." @default.
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• W2023854813 date "2009-10-19" @default.
• W2023854813 modified "2023-09-26" @default.
• W2023854813 title "Reactivity of Methoxy Species toward CO on Keggin 12-H₃PW₁₂O₄₀: A Study with Solid State NMR" @default.
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• W2023854813 doi "https://doi.org/10.1021/jp906888m" @default.
• W2023854813 hasPublicationYear "2009" @default.
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