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- W2023862608 abstract "A rapid and accurate method was developed for the determination of the enantiomeric composition of amphetamine preparations. Amide derivatives of the amphetamine enantiomers are first formed by using achiral 2-naphthoyl chloride. The resulting enantiomeric amides are then chromatographed on a commercially available chiral stationary phase. The capacity factors (k') of (-)- and (+)-2-naphthoylamphetamine are 20 and 22, respectively, and the separation factor (alpha) for the two enantiomers is 1.08. The method allows detection of as little as 0.5% of the (-)-enantiomer in (+)-amphetamine and is applicable to both bulk drug and single-tablet analyses." @default.
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- W2023862608 date "1984-08-01" @default.
- W2023862608 modified "2023-09-23" @default.
- W2023862608 title "Liquid Chromatographic Chiral Stationary Phases in Pharmaceutical Analysis: Determination of Trace Amounts of the (-)-Enantiomer in (+)-Amphetamine" @default.
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- W2023862608 doi "https://doi.org/10.1002/jps.2600730835" @default.
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