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- W2023897492 abstract "Herein, we report the preparation of thermo-responsive polymers in a green medium. The white, dry, fine powders were obtained directly from the cross-linking polymerization of N-isopropylacrylamide (NIPA) in supercritical carbon dioxide (scCO2) at pressures ranging from 10 to 28 MPa utilizing ethylene glycol dimethacrylate (EGDMA) as a cross-linker. The effects of reaction pressure, cross-linker ratio, initiator concentration, and reaction time were investigated. In the presence of this cross-linker (26.4% w/w), much smaller poly(N-isopropylacrylamide) (PNIPA) microgels (<0.2 µm diameter) were formed, and it was shown that the particle size and the morphology of the polymer were strongly dependent on the cross-linker ratio in scCO2. Copyright © 2009 John Wiley & Sons, Ltd." @default.
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- W2023897492 date "2009-06-26" @default.
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- W2023897492 title "Synthesis of thermo-responsive microgels in supercritical carbon dioxide using ethylene glycol dimethacrylate as a cross-linker" @default.
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- W2023897492 doi "https://doi.org/10.1002/pat.1440" @default.
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