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- W2023961930 abstract "C9H7N3, M(r) = 157.2, monoclinic, P2(1)/c, a = 7.145 (8), b = 10.866 (5), c = 11.006 (6) angstrom, beta = 107.53 (6)-degrees, V = 814.8 angstrom 3, Z = 4, D(x) = 1.281 g cm-3, lambda(Mo K-alpha) = 0.71069 angstrom, mu = 0.76 cm-1, F(000) = 328, T = 293 K, R = 0.048 for 1023 observed reflections. The reaction of alpha,beta-unsaturated aldehydes with malononitrile is a synthetic method leading to 2-alkoxy-3-cyanopyridines. In this reaction a minor product is also obtained having an isophthalonitrilic structure. Thus, the title compound comes from the reaction between methacrolein and malononitrile. The X-ray determination confirms the chemical structure. The amino group evenly releases electronic charge towards both nitrile groups. Bond distances, as well as NMR and IR data, are in agreement with this assumption." @default.
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- W2023961930 date "1992-01-15" @default.
- W2023961930 modified "2023-09-26" @default.
- W2023961930 title "Structure of 2-amino-5-methylisophthalonitrile" @default.
- W2023961930 doi "https://doi.org/10.1107/s010827019100865x" @default.
- W2023961930 hasPublicationYear "1992" @default.
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