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- W2024005325 abstract "Abstract High-performance Ca 3 Co 4 O 9 thermoelectric ceramic has been prepared from a Ca 1− x Co x O/Ca y Co 1− y O divorced eutectic structure produced by a directional melt-grown using the laser floating zone technique. This material has been grown at very high solidification rate in order to produce a very fine microstructure to reduce the necessary annealing time to recover the Ca 3 Co 4 O 9 thermoelectric phase as the major one. As-grown and annealed samples were microstructurally characterized to determine the phases and estimate the extent of Ca 3 Co 4 O 9 formation with time and related with their thermoelectric performances. The optimum annealing time, 72 h, has been determined by the maximum power factor value (about 0.42 mW K −2 m −1 ), which is around the best values reported in textured materials (∼0.40 mW K −2 m −1 ). This high power factor outcome from the high Ca 3 Co 4 O 9 phase content, apparent density and Co 3+ /Co 4+ relationship determinations performed in the present work." @default.
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- W2024005325 date "2013-09-01" @default.
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- W2024005325 title "Preparation of high-performance Ca3Co4O9 thermoelectric ceramics produced by a new two-step method" @default.
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- W2024005325 doi "https://doi.org/10.1016/j.jeurceramsoc.2013.01.029" @default.
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