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- W2024104268 abstract "Abstract Polymethyl methacrylates and polystyrenes have been prepared by the free radical polymerization of the monomers in the presence of α,α′‐diphenyl‐β‐picryl hydrazine. The polymethyl methacrylates were yellow and on treatment with lead dioxide became violet and showed electron paramagnetic resonance (e.p.r.) absorption. It is concluded from the e.p.r. spectra that the polymethyl methacrylates contain diphenylpicryl hydrazine end groups, which, on oxidation, form diphenylpicryl hydrazyl groups. The e.p.r. spectrum of a 5% benzene solution of a polymethyl methacrylate indicates that, in this solution, the correlation time for reorientation of the free‐radical end groups is less than 10 −8 sec. Polystyrenes prepared in this manner were also yellow, but were unaffected by lead dioxide." @default.
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- W2024104268 date "1961-02-01" @default.
- W2024104268 modified "2023-10-16" @default.
- W2024104268 title "A study by E.P.R. of the reaction between polymer radicals and α,α′-diphenyl-β-picryl hydrazine" @default.
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- W2024104268 doi "https://doi.org/10.1002/pol.1961.1204915205" @default.
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