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- W2024150744 endingPage "1419" @default.
- W2024150744 startingPage "1403" @default.
- W2024150744 abstract "Single crystals of three new lanthanide oxalate complexes, (CN3H6)2[Nd(H2O)]2(C2O4)4⋅3H2O I, [N(CH3)4][Nd2(H2O)3](C2O4)3.5⋅4H2O II and [N(CH3)4][Yb(C2O4)2] III, have been synthesized hydrothermally in presence of either the guanidinium or tetramethylammonium TMA ions. A relevant feature of III is the complete absence of water. For all the complexes, the three-dimensional framework structure is built up by the connections of the lanthanide and the oxalate units, forming cavities and channels where the guest species, guanidinium and TMA ions and free water molecules, are localized. Thus, the above complexes present a very open architecture. For I and II, the neodymium atoms are 9-coordinated, forming a distorted monocapped square antiprism while for III, the ytterbium atom is 8-coordinated forming a quite regular dodecahedron. For I, the dehydration process is partially reversible. All the complexes will be characterized by infrared spectroscopy and thermal analysis. I has been extended to other lanthanide forming a family, Ln = La–Eu." @default.
- W2024150744 created "2016-06-24" @default.
- W2024150744 creator A5026222214 @default.
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- W2024150744 date "2004-12-01" @default.
- W2024150744 modified "2023-09-27" @default.
- W2024150744 title "Synthesis and crystal structure of three-dimensional open-framework lanthanide oxalates containing either the guanidinium or tetramethylammonium ions" @default.
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- W2024150744 doi "https://doi.org/10.1016/j.solidstatesciences.2004.07.019" @default.
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