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- W2024168164 abstract "ABSTRACT A novel hydrodynamic sequential injection (HSI) spectrophotometric system for determination of manganese was developed. It is based on the complexation of Mn(II) with formaldoxime in basic solution (pH ≥ 10) to produce product that could be monitored spectrophotometrically at 450 nm. Based on the HSI concept, both sample and reagents were aspirated through solenoid valves to fill a defined volumes conduit between 3-way connectors connected in series, forming stacked zones of solutions similar to those in normal SI. The concept was successfully demonstrated for manganese determination. A linear calibration graph over a range of 0.5 to 30 mg L−1 Mn(II) with a detection limit of 0.2 mg L−1 was obtained. Relative standard deviations for 11 replicated injections of 5 and 20 mg Mn L−1 were 5.6% and 2.4%, respectively. A sample throughput of 45 h−1 was achieved. The results from investigation of exchangeable manganese in soil samples by the developed method were found to be in good agreement with the re..." @default.
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- W2024168164 date "2008-08-15" @default.
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- W2024168164 title "Hydrodynamic Sequential Injection Spectrophotometric System for Determination of Manganese in Soil" @default.
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- W2024168164 doi "https://doi.org/10.1080/00387010802134553" @default.
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