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- W2024169917 abstract "Abstract NiWO 4 powders have been synthesized by reaction between NiCl 2 and Na 2 WO 4 aqueous solutions and following calcinations at different temperatures. X-ray diffraction and scanning electron microscopy analysis were used to characterize the powders. Single phase NiWO 4 powders were formed above a calcining temperature of 600 °C. X-ray diffraction analysis indicated that the NiWO 4 powders had a monoclinic structure and particle size of 26.8 nm and 30.3 nm for calcining temperatures of 600 °C and 700 °C, respectively. A little increase in intensity of the X-ray diffraction peaks was observed when increasing the calcining temperature from 600 °C to 700 °C. Scanning electron microscopy indicated that powders had uniform and very small particle size. The powders showed a broad blue-green emission band. The broad band of NiWO 4 powders calcined at 600 °C consisted of 423.2 nm (2.93 eV), 487.3 nm (2.54 eV) and two weak bands at 447.0 nm (2.77 eV), and 532.0 nm (2.33 eV). Small shifts in the peaks of excitation and luminescence and small increases in intensities were observed when increasing calcining temperature to 700 °C. The films were deposited using the sol-gel method and using the precipitate as starting materials. The deposited films showed a similar blue-green emission to that of the powders." @default.
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- W2024169917 date "2010-03-01" @default.
- W2024169917 modified "2023-10-15" @default.
- W2024169917 title "Luminescence of aqueous reactions derived NiWO4 powders and sol-gel deposited films" @default.
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- W2024169917 doi "https://doi.org/10.3139/146.110280" @default.
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