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- W2024172011 abstract "Atom efficient reactions of 3-ferrocenyl-2H-azaphosphirene complex 1 using a newly developed acid/base ring expansion protocol are presented. Consecutive reaction of 1 in the presence of dimethyl cyanamide with triflic acid and triethylamine yielded the selective formation of 2H-1,4,2-diazaphosphole complex 3. The same protocol using acetone, benzaldehyde and ferrocenyl aldehyde afforded 1,3,5-oxazaphosphol-3-ene complexes 4, 5a,b and 6a,b, the latter as mixtures of diastereomers, which could be separated. Apart from NMR, IR and UV/vis spectroscopic data, the single-crystal X-ray structures of complexes 3, 4 and 6a are discussed." @default.
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- W2024172011 date "2010-01-01" @default.
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- W2024172011 title "Developing click reactions of a 3-ferrocenyl-2H-azaphosphirene complex" @default.
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- W2024172011 doi "https://doi.org/10.1039/c0dt00730g" @default.
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