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- W2024202017 abstract "Transmetallation reactions of ortho-mercurated iminophosphoranes (2-ClHgC6H4)Ph2PNR with [AuCl4]− gives new cycloaurated iminophosphorane complexes of gold(III) (2-Cl2AuC6H4)Ph2PNR [R = (R,S)- or (S)-CHMePh, p-C6H4F, tBu], characterised by NMR and IR spectroscopies, ESI mass spectrometry and an X-ray structure determination on the chiral derivative R = (S)-CHMePh. The chloride ligands of these complexes can be readily replaced by the chelating ligands thiosalicylate and catecholate; the resulting derivatives show markedly higher anti-tumour activity versus P388 murine leukaemia cells compared to the parent chloride complexes. Reaction of (2-Cl2AuC6H4)Ph2PNPh with PPh3 results in displacement of a chloride ligand giving the cationic complex [(2-Cl(PPh3)AuC6H4)Ph2PNPh]+, indicating that the PN donor is strongly bonded to the gold centre." @default.
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- W2024202017 date "1981-01-01" @default.
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- W2024202017 title "Synthesis and reactivity of dichloro 2-(phenylazo)phenyl gold(III)" @default.
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- W2024202017 doi "https://doi.org/10.1016/s0020-1693(00)95453-7" @default.
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