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• W2024244579 abstract "Five new intramolecularly coordinated aluminum species, whose molecular structures have been elucidated in solution by NMR spectroscopy and in the solid state by single crystal X-ray analysis, are described. All species are equipped with a trisyl-based ligand with a pyridyl donor group [Pytsi stands for -C(SiMe 3 ) 2 SiMe 2 (2-C 5 H 4 N)]. While the compound (Pytsi)AlMeCl was accessible either from Li(THF)(Pytsi) and MeAlCl 2 or from (Pytsi)AlCl 2 and LiMe, the tert-butyl derivative (Pytsi)AltBuCl could only be obtained from Li(THF)(Pytsi) and tBuAlCl 2 . Attempted synthesis of (Pytsi)AltBuCl from (Pytsi)AlCl 2 and LitBu or from (Pytsi)AlCl 2 and tBuMgCl failed. Three other compounds (3-5) were synthesized and can be described as derivatives of (Pytsi)AlMe 2 with additional groups in the ortho position of the pyridyl group. Compound 3 carried a Me group in the ortho position, while compounds 4 and 5 were equipped with Ph and 2,6-diisopropylphenyl moieties, respectively.Key words: aluminum, trisyl ligands, methyl alanes." @default.
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• W2024244579 date "2007-07-01" @default.
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• W2024244579 title "Synthesis and characterization of intramolecularly coordinated alanes with new sterically demanding trisyl-based ligands" @default.
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• W2024244579 doi "https://doi.org/10.1139/v07-063" @default.
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