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- W2024251617 abstract "Graphite ferric chloride, C 12 FeCl 3 , was prepared by heating anhydrous ferric chloride with graphite at 305 °C. The purified compound containing 53% ferric chloride was not attacked by hot 6 N hydrochloric acid and gave an X-ray diffraction pattern which was distinctly different from that of either graphite or ferric chloride. The separation of the graphite layer-planes was increased from 3.36 to 9.4 Å by the intercalation of the ferric chloride molecules.Tests for exchange between C 12 FeCl 3 and Fe +++ ion were made using radioactive Fe 59 . In no instance was any measurable exchange observed. The compound was subjected to neutron irradiation and the Szilard–Chalmers yield of separable activity calculated and identified. The separated portion contained less than 1% of the total activity and consisted of Fe 59 , P 32 , and S 35 .The lack of exchange and the low Szilard–Chalmers yield are attributed to the formidable steric hindrance effects which result from the stacked layer structure for graphite ferric chloride." @default.
- W2024251617 created "2016-06-24" @default.
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- W2024251617 date "1956-11-01" @default.
- W2024251617 modified "2023-09-25" @default.
- W2024251617 title "RADIOCHEMICAL STUDIES OF GRAPHITE FERRIC CHLORIDE" @default.
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- W2024251617 doi "https://doi.org/10.1139/v56-206" @default.
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