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- W2024273338 abstract "The aim of this study was to introduce a new method for determining the surface composition and surface order of PP/EPDM (propylene/ethylene–diene–monomer rubber) blends, based on surface-enhanced infrared spectroscopy. PP/EPDM blends were characterized by Fourier transfer IR–attentuated total reflectance (FTIR-ATR) using two different internal reflection elements, Ge and KRS-5. These elements provide information at different depths and show differences in relative band intensities. A linear relationship between the ratio of the bands at 2850 and 2920 cm−1 EPDM content was obtained when well-defined compositions of PP and EPDM mixtures were used. Changes in crystallinity were measured by the ratio of the bands at 2959 and 2951 cm−1. For comparison, bands in the lower region of the spectrum and DSC and WAXS measurments were used. It was shown by two calibration methods that FTIR-ATR can provide information on surface composition and surface crystallinity at very low penetration depths. This new method indicates that injection-molded sample show a lower surface order and lower EPDM content at the surface than is seen in bulk. © 1993 John Wiley & Sons, Inc." @default.
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- W2024273338 date "1993-10-01" @default.
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- W2024273338 title "Physical modifications of propylene/ethylene–propylen–diene–monomer rubber surfaces. I. Determination of surface composition and surface order by fourier transform infrared–attenuated total reflectance" @default.
- W2024273338 doi "https://doi.org/10.1002/polb.1993.090311106" @default.
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