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- W2024278766 abstract "The role of ancillary ligands, namely imidazole (im), pyridine (py), 2,2′-bipyridine (bpy) and 1,10-phenanthroline (phen) in the assembly of copper(II) dipicolinate complexes are presented. Mononuclear complexes are observed in the case of monodentate ligands. The mononuclear complex [Cu(im)3L]·4H2O (1) (L = dipicolinate anion) has a distorted octahedral structure with Z′ = 2, whereas [CuL(py)(H2O)]·2H2O (2) adopts distorted square pyramidal geometry. The bidentate ligands bpy and phen favor the formation of dinuclear complexes. The dinuclear complex [CuL(bpy)(μ-L)Cu(bpy)(H2O)]·9H2O (3) has one carbonyl oxygen atom of a carboxylate group of dipicolinate acting as a bridging ligand to the copper site that is devoid of a coordinated water molecule. The complex has an angle of 83.55° between the plane of L and bpy attached to one copper site, whereas it has an angle of 78.13° between the plane L and bpy attached to the other copper site. A 1,10-phenanthroline containing dinuclear copper(II) dipicolinate complex, [Cu(phen)(H2O)(μ-L)Cu(phen)2][CuL2]·12H2O (4), has been structurally characterized. It has an unusual carboxylate bridge." @default.
- W2024278766 created "2016-06-24" @default.
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- W2024278766 date "2012-01-01" @default.
- W2024278766 modified "2023-09-26" @default.
- W2024278766 title "Assembling of copper(II) dipicolinate complexes" @default.
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- W2024278766 doi "https://doi.org/10.1016/j.poly.2011.09.039" @default.
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