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- W2024282672 abstract "ABSTRACT The mechanism of intercalation of piperidine in α-hafnium phosphate, Hf(HPO4;V) 2H2O (dooz = 7.6 [Adot]) and γ-hafnium phosphate, Hf(P04)(H2P04) 2H20 (doo2 - 12.1 [Adot]), has been investigated by the batch method. Saturated phases were not obtained. The reactions take place stepwise with the final formation of the compounds Hf(HPO4) 2 C5H11N H2O and Hf[P04)(H2P04)C5 H11 N 2H20. In the α-HfP case, no intermediate phases have been detected but in the γ-HfP case, a new phase, Hf(PO4)(H2PO4)0.38C5H11N 2H2O, was isolated The characterization of the intercalates was made by chemical and thermal analysis, X-ray diffraction and 1R spectroscopy. Materials with a monolaminar arrangement of amine molecules in the phosphate interlayer region were obtained and the results are compared to those described using different intercalation conditions." @default.
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- W2024282672 date "1999-09-01" @default.
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- W2024282672 title "STEPWISE INTERCALATION OF PIPERJDINE IN LAYERED α- AND γ- HAFNIUM PHOSPHATE" @default.
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- W2024282672 doi "https://doi.org/10.1080/07366299908934652" @default.
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