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• W2024284690 abstract "A potentially pentadentate hydrazone ligand, N ′-[1-(pyrazin-2-yl)ethylidene]nicotinohydrazide (H L ), was prepared from the condensation reaction of nicotinohydrazide and acetylpyrazine. Reactions of H L with MnCl 2 , Mn(CH 3 COO) 2 and Cd(CH 3 COO) 2 afforded three metal complexes, namely dichlorido{ N ′-[1-(pyrazin-2-yl-κ N 1 )ethylidene]nicotinohydrazide-κ 2 N ′, O }manganese(II), [MnCl 2 (C 12 H 11 N 5 O)], (I), bis{ N ′-[1-(pyrazin-2-yl-κ N 1 )ethylidene]nicotinohydrazidato-κ 2 N ′, O ]manganese(II), [Mn(C 12 H 10 N 5 O) 2 ], (II), and poly[[(acetato-κ 2 O , O ′){μ 3 - N ′-[1-(pyrazin-2-yl-κ 2 N 1 : N 4 )ethylidene]nicotinohydrazidato-κ 3 N ′, O : N 1 }cadmium(II)] chloroform disolvate], {[Cd(C 12 H 10 N 5 O)(CH 3 COO)]·2CHCl 3 } n , (III), respectively. Complex (I) has a mononuclear structure, the Mn II centre adopting a distorted square-pyramidal coordination. Complex (II) also has a mononuclear structure, with the Mn II centre occupying a special position ( C 2 symmetry) and adopting a distorted octahedral coordination environment, which is defined by two O atoms and four N atoms from two N ′-[1-(pyrazin-2-yl)ethylidene]nicotinohydrazidate ( L − ) ligands related via a crystallographic twofold axis. Complex (III) features a unique three-dimensional network with rectangular channels, and the L − ligand also serves as a counter-anion. The coordination geometry of the Cd II centre is pentagonal bipyramidal. This study demonstrates that H L , which can act as either a neutral or a mono-anionic ligand, is useful in the construction of interesting metal–organic compounds." @default.
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• W2024284690 date "2015-01-17" @default.
• W2024284690 modified "2023-10-18" @default.
• W2024284690 title "Mononuclear and three-dimensional metal complexes based on a multidentate hydrazone ligand" @default.
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• W2024284690 doi "https://doi.org/10.1107/s2053229615000698" @default.
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