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- W2024316860 abstract "Stereospecific polycondensation of trityl ethers of trisaccharide 1,2-O-cyanoethylidene derivatives (1 and 3) followed by deprotection afforded regular heteropolysaccharides (2 and 4) built up of repeating trisaccharide units, viz (→6)-β-d-Manp-(1→4)-α-l-Rhap-(1→3)-β-Galp-(1 → and → 6);-α-d-Manp-(1→4)-α-l-Rhap-(1→3)-β-d-Galp-(l →, respectively. The synthetic polysaccharide 2 exhibited the high biological specificity of the natural one, whilst its analogue 4 was found to be practically inactive. The necessary monomers for polycondensation, 1 and 3, were obtained from the respective trisaccharide α-decaacetates (5 and 7) by successively converting them into glycosyl bromides and 1,2-O-cyanoethylidene derivatives which, in turn, were subjected to deacylation followed by tritylation." @default.
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- W2024316860 date "1981-01-01" @default.
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- W2024316860 title "Synthesis of the O-antigenic polysaccharide of Salmonella newington and of its analogue differing in configuration at the only glycosidic centre" @default.
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- W2024316860 doi "https://doi.org/10.1016/0040-4020(81)85050-8" @default.
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