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- W2024339929 abstract "ABSTRACT This study devoted to V1'IR spectroscopy of monolayers spread at the air/water interface is, to our knowledge, the first onepresenting complete mid-infrared monolayer spectra devoided of strong water vapor absorptions. This has been possible by usingthe PM-IRRAS method combining polarization modulation with two channel simultaneous acquisition. Due to its differentialcharacter, the detected signal is not sensitive to the isotropic absorptions of the sample environment. From theoretical simulationsand experiments, the best angle of incidence was found to be near 76° for the detection of intrasurface as well as out of surfacetransition moments. Under these experimental conditions, the absorption bands of the monolayer appear upwards or downwards inthe normalized diffemce (covered vs uncovered) PM-IRRAS spectra depending on the orientation (parallel or perpendicular) of theiriransition moments with respect to the interface. Application to the study of a close-packed arachidate monolayer has allowed fullobservation of its vibrational modes. Theoretical simulation of these spectra provides evidence of a symmetrical anchoring of thepolar head groups and of a preferential perpendicular orientation of the alkyl chains with respect to the water surface." @default.
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- W2024339929 date "1994-01-31" @default.
- W2024339929 modified "2023-09-23" @default.
- W2024339929 title "Polarization modulation FTIR spectroscopy of a spread monolayer at the air-water interface" @default.
- W2024339929 doi "https://doi.org/10.1117/12.166641" @default.
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