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• W2024345932 abstract "The synthesis of the n = 5 and n = 6 members of the HgBa2Can−1CunO2n+2+δ family are reported. Bulk samples containing either Hg-1245 or Hg-1256 as major phases were synthesized using the high-pressure high-temperature technique at 920°C and 18 kbar. The as-synthesized phases (a = 3.8547(3) Å, c = 22.156(5) Å for n = 5 and a = 3.8516(1) Å, c = 25.232(6) Å for n = 6) exhibited Tc with onsets of about 100 K. They were characterized by X-ray powder diffraction, transmission electron microscopy and AC susceptibility measurements. Heat treatments increased the Tc onset to 110 K for n = 5 and to 107 K for n = 6. These phases with high n are more inert to thermal annealing under different atmospheres than the members with smaller n. Only strong oxidizing {P(O2) ≥ 500 bar} or reducing {Ar/400 °C} condition can induce significant Tc variations." @default.
• W2024345932 created "2016-06-24" @default.
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• W2024345932 date "1996-01-01" @default.
• W2024345932 modified "2023-10-17" @default.
• W2024345932 title "High-pressure synthesis and heat treatments of the HgBa2Ca4Cu5O12+δ and HgBa2Ca5Cu6O14+δ phases" @default.
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• W2024345932 doi "https://doi.org/10.1016/0921-4534(95)00635-4" @default.
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