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• W2024391292 endingPage "1168" @default.
• W2024391292 startingPage "1159" @default.
• W2024391292 abstract "The `P2N' mixed donor ligand 2-(diphenylphosphino)-N-[2-(diphenylphosphino)benzylidene]benzeneamine (PNCHP) reacts with [MCl2(1,5-cyclooctadiene)] and [M(CH3)Cl(1,5-cyclooctadiene)] to give the complexes [M(PNCHP-κ3P,N,P)Cl]Cl (M=Pt or Pd) and [Pd(PNCHP-κ3P,N,P)(CH3)]Cl, respectively. The ionic chloride can be exchanged with BF4− by reaction with AgBF4. Abstraction of the covalent chloride with AgBF4 in the presence of acetonitrile yields [Pt(PNCHP-κ3P,N,P)(CH3CN)]2+. The acetonitrile ligand of this dication can be substituted with a variety of ligands to afford complexes of the type, [Pt(PNCHP-κ3P,N,P)L]2+ (L=the monodentate ligands: triphenylphosphine, 2-picoline, 3-picoline or the chelate ligands: 1,10-phenanthroline, 2,2′-bipyridine, bis(diphenylphosphino)ethane, 2,2′:6′,2″-terpyridine). The latter ligands all bind in a bidentate fashion to give five-coordinate complexes. The compounds have been characterised by spectroscopic and analytical means. The single crystal structures of the four-coordinate complexes, [Pt(PNCHP-κ3P,N,P)Cl]Cl and [Pt(PNCHP-κ3P,N,P)(PPh3)](BF4)2, and the five-coordinate complexes, [Pt(PNCHP-κ3P,N,P)L](BF4)2 (L=1,10-phenanthroline and 2,2′:6′,2″-terpyridine), have been determined." @default.
• W2024391292 created "2016-06-24" @default.
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• W2024391292 date "2004-04-01" @default.
• W2024391292 modified "2023-10-17" @default.
• W2024391292 title "Platinum(II) and palladium(II) complexes containing a mixed donor `P2N' multidentate ligand" @default.
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• W2024391292 doi "https://doi.org/10.1016/j.poly.2004.01.015" @default.
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