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- W2024392776 abstract "We have prepared a full series of 1,6-anhydro-2,3,4-trideoxy-4-fluoro-2,3-epimino-β-d-hexopyranoses. The key step was the reaction of azido sulfonates possessing a free C-4 hydroxyl with DAST and subsequent LiAlH4 reduction. Nucleophilic displacement of the hydroxyl activated by DAST proceeded without rearrangement and with moderate to good yields. A convenient synthesis of d-mannoepimine from a readily available 3-benzylamino derivative was also developed." @default.
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- W2024392776 date "2010-04-16" @default.
- W2024392776 modified "2023-10-18" @default.
- W2024392776 title "Synthesis of All Configurational Isomers of 1,6-Anhydro-2,3,4-trideoxy-2,3-epimino-4-fluoro-β-<scp>d</scp>-hexopyranoses" @default.
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- W2024392776 doi "https://doi.org/10.1021/jo1000912" @default.
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