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• W2024429511 startingPage "12507" @default.
• W2024429511 abstract "The structural development of the ordered intermetallic compounds ${mathit{T}}_{3}$${mathit{X}}_{2}$ (T=Ni,Fe,Mn; X=Sn,Ge) upon mechanical milling was investigated by x-ray diffraction, magnetic measurements, and subsequently by differential scanning calorimetry (DSC). It is found that the magnetization at 4.2 K increases continuously with increasing milling time in ferromagnetic ${mathrm{Ni}}_{3}$${mathrm{Sn}}_{2}$ and ${mathrm{Fe}}_{3}$${mathrm{Ge}}_{2}$. In contrast, in ferrimagnetic ${mathrm{Mn}}_{3}$${mathrm{Sn}}_{2}$ it decreases. The unit-cell volume of both ${mathrm{Mn}}_{3}$${mathrm{Sn}}_{2}$ and ${mathrm{Fe}}_{3}$${mathrm{Ge}}_{2}$ continuously increases. These results are explained well in terms of a special type of atomic disorder: redistribution of transition-metal atoms over two different types of transition-metal sites, induced by ball milling. Exothermic heat effects corresponding to atomic reordering are observed in the DSC scans of ${mathrm{Mn}}_{3}$${mathrm{Sn}}_{2}$ and ${mathrm{Fe}}_{3}$${mathrm{Ge}}_{2}$ as well as ${mathrm{Ni}}_{3}$${mathrm{Sn}}_{2}$ after various periods of milling. The heat evolved in the atomic reordering process increases gradually with milling time. After long-time milling all physical parameters tend to become constant. After prolonged periods of milling, a phase transformation in ${mathrm{Ni}}_{3}$${mathrm{Sn}}_{2}$ from the orthorhombic-structure low-temperature phase (LTP) to the hexagonal-structure high-temperature phase (HTP) is observed accompanied by a sharp increase in magnetization. ${mathrm{Mn}}_{3}$${mathrm{Sn}}_{2}$ and ${mathrm{Fe}}_{3}$${mathrm{Ge}}_{2}$ remain in the hexagonal structure.The exothermic heat effect corresponding to the phase restoration of the ball-milled metastable HTP to the original equilibrium LTP is evident from DSC scans of ${mathrm{Ni}}_{3}$${mathrm{Sn}}_{2}$ after long milling periods. The occurrence of the ball-milling-induced phase transformation in ${mathrm{Ni}}_{3}$${mathrm{Sn}}_{2}$ is also confirmed by a comparison of the ball-milled phase to the high-temperature phase obtained by rapid quenching. The excellent agreement of all experimental results obtained by different techniques proves that by mechanical milling well-defined metastable states are generated in these B8-like compounds and that atomic disorder is the main source of energy storage during ball milling of intermetallic compounds. The particular type of atomic disorder in these B8-like compounds cannot be obtained by rapid quenching from high temperatures." @default.
• W2024429511 created "2016-06-24" @default.
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• W2024429511 date "1994-05-01" @default.
• W2024429511 modified "2023-09-26" @default.
• W2024429511 title "Atomic disorder and phase transformation in intermetallic compounds of the type<mml:math xmlns:mml=http://www.w3.org/1998/Math/MathML display=inline><mml:mrow><mml:msub><mml:mrow><mml:mi mathvariant=italic>T</mml:mi></mml:mrow><mml:mrow><mml:mn>3</mml:mn></mml:mrow></mml:msub></mml:mrow></mml:math><mml:math xmlns:mml=http://www.w3.org/1998/Math/MathML display=inline><mml:mrow><mml:msub><mml:mrow><mml:mi mathvariant=italic>X</mml:mi></mml:mrow><mml:mrow><mml:mn>2</mml:mn></mml:mrow…" @default.
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• W2024429511 doi "https://doi.org/10.1103/physrevb.49.12507" @default.
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