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• W2024449332 abstract "Abstract Chemical modification reactions of alkyne containing polyHEMA‐based macroporous network structures (cryogels) by Cu(I) catalyzed azide‐alkyne ‘click’ cycloaddition reactions and their monitoring and quantification with high‐resolution magic angle spinning (hr‐MAS) NMR spectroscopy are reported. Complete conversion is obtained when benzylazide is reacted with the grafted alkyne function, but only partial conversion is observed when using azide‐modified poly(ethylene glycol) (PEG‐N 3 ). Subsequent addition of benzylazide consumes all remaining alkyne groups. All chemical modifications are easily monitored at each stage using hr‐MAS NMR spectroscopy. The alkyne functionality and the resulting triazole ring provide well resolved 1 H resonances to monitor and quantify the progress of such ‘click’ reactions in general. magnified image" @default.
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• W2024449332 date "2009-07-28" @default.
• W2024449332 modified "2023-10-17" @default.
• W2024449332 title "‘Click’ Functionalization of Cryogels Conveniently Verified and Quantified Using High-Resolution MAS NMR Spectroscopy" @default.
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• W2024449332 doi "https://doi.org/10.1002/marc.200900087" @default.
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