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- W2024481411 abstract "High-performance liquid chromatography-atmospheric pressure chemical ionization mass spectrometry was used to identify flavone aglycones and glycosides in soybean pods. Tandem mass spectrometry (MS-MS and MS-MS-MS) and photodiode array detection were also utilized in flavone characterization. A total of seven flavone aglycones and glycosides were identified. Among them three flavone aglycones--apigenin, 7,4'-dihydroxyflavone, and luteolin--and two flavone glycosides--apigenin-7-O-beta-D-glucoside, and luteolin-7-O-beta-D-glucoside--were unambiguously identified based on their abundant (M+H)+ ions, UV spectra, retention time, and tandem mass spectrometric analysis compared with authentic standards. The tentative identification of two flavone glycosides as 7,4'-dihydroxyflavone-7-O-beta-D-glucoside and apigenin-7-O-beta-D-glucoside-6-O-malonate was based on UV spectra, (M+H)+ ions, and tandem mass spectrometry. This is the first report identifying flavone aglycones and glycosides in soybean pods." @default.
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- W2024481411 date "2003-03-01" @default.
- W2024481411 modified "2023-09-23" @default.
- W2024481411 title "Identification of flavone aglycones and glycosides in soybean pods by liquid chromatography–tandem mass spectrometry" @default.
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- W2024481411 doi "https://doi.org/10.1016/s0021-9673(03)00209-7" @default.
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