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- W2024563679 abstract "P4O7S wurde erstmals dargestellt und durch Röntgenstrukturanalyse an Einkristallen sowie 31P-NMR (Lösung und MAS-Festkörper) charakterisiert (P1; a = 687,2(1); b = 718,2(1); c = 809,1(1) pm; α = 92,58(1)°; β = 104,43(1)°; γ = 94,82(2)°; 2 907 Diffraktometerdaten; R1 = 0,030; wR2 = 0,102). Der unterschiedliche Einfluß von terminalem Sauerstoff und Schwefel auf die Geometrie des Käfigs in P4O7S wird diskutiert. Syntheses and Characterization of P4O7S P4O7S was synthesized for the first time and characterized by X-ray structure determination (single-crystal methods) and 31P-n.m.r. (solution and MAS-solid) (P1; a = 687.2(1); b = 718.2(1); c = 809.1(1) pm; α = 92.58(1)°; β = 104.43(1)°; γ = 94.82(2)°; 2 907 diffractometer data; R1 = 0.030; wR2 = 0.102). The different influences of terminally bound oxygen and sulfur on the geometry of the P4O6 cage are discussed." @default.
- W2024563679 created "2016-06-24" @default.
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- W2024563679 date "1995-03-01" @default.
- W2024563679 modified "2023-09-27" @default.
- W2024563679 title "Darstellung und Charakterisierung von P4O7S" @default.
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- W2024563679 doi "https://doi.org/10.1002/zaac.19956210325" @default.
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