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- W2024565536 abstract "A detailed analysis of the three-phase structure of poly(L-lactic acid) was performed by temperature-modulated differential scanning calorimetry upon quasi-isothermal and non-isothermal crystallizations. The TMDSC analyses revealed that the relative amounts of the three fractions of poly(L-lactic acid) depend on the temperature at which crystallization occurs. It was found that rigid amorphous fraction grows in parallel with crystalline phase during quasi-isothermal crystallization at 90 °C, whereas at Tc = 130 °C it starts to appear approximately in correspondence with secondary crystallization. At Tc = 135 °C RAF practically does not develop. The results prove that RAF development during crystallization depends on the mobility of the chains. The temperature of complete devitrification at 10 °C min−1 seems to be 130 °C: this temperature could be the limit for the formation and the disappearance of rigid amorphous fraction in the PLLA sample analyzed in the present study." @default.
- W2024565536 created "2016-06-24" @default.
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- W2024565536 date "2011-08-01" @default.
- W2024565536 modified "2023-10-14" @default.
- W2024565536 title "Crystalline, mobile amorphous and rigid amorphous fractions in poly(L-lactic acid) by TMDSC" @default.
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- W2024565536 doi "https://doi.org/10.1016/j.tca.2010.12.024" @default.
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