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- W2024583329 abstract "The method described of elemental analysis of carbon, hydrogen, and nitrogen is based on the oxidation pyrolysis of sample in a tube containing Dumas filling; dilution of the combustion products with helium in a cylindrical chamber with pneumatically controlled piston; setting of the diffusional equilibrium at constant state conditions in the chamber; chromatographic separation of the nitrogen, carbon dioxide, and water by the frontal technique; and detection of the above substances by a katharometer. Two records, those of sorption and desorption, are obtained from a single sample. The use of both records makes it possible to decrease considerably the error of determination, brought about by the Chromatographic, detection, and recording parts of the instrument. The expanding of the detector signal over several recorder scales is used to an advantage. The method provides for the combustion under both static and dynamic conditions, as well as work on submicro-, micro-, and, if need be, semimicroscales." @default.
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- W2024583329 date "1970-09-01" @default.
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- W2024583329 title "Simultaneous determination of carbon, hydrogen, and nitrogen by means of gas chromatography" @default.
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- W2024583329 doi "https://doi.org/10.1016/0026-265x(70)90123-2" @default.
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