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- W2024607637 abstract "A suite of twenty-one bituminous coal samples from Ohio were analyzed by differential scanning calorimetry (DSC) and non-isothermal thermogravimetry (TG) techniques. Three regions of endothermic activity may be distinguished in the DSC scans in an inert atmosphere. The first peak (25–150°C) corresponds to loss of moisture from the coal, a second, very broad endotherm peaking in the range 400–500°C corresponds to devolatilization of the organic matter and a partially resolved endotherm at temperatures above 550°C probably corresponds to cracking and coking processes subsequent to the pyrolysis step. Evidence obtained from experiments with sealed pans suggest an autocatalytic effect exerted by the pyrolysis products. The use of the DSC technique to quantify the volatile matter content of coal seems less reliable than the proximate analyses obtained from non-isothermal TG in inert and O2 atmospheres. Good agreement with ASTM values is observed by the latter method for a range of volatile matter and ash content." @default.
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- W2024607637 date "1982-03-01" @default.
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- W2024607637 title "Thermal analyses of Ohio bituminous coals" @default.
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- W2024607637 doi "https://doi.org/10.1016/0040-6031(82)85024-7" @default.
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