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• W2024641109 startingPage "12107" @default.
• W2024641109 abstract "A minor enantiomer recycling one-pot procedure employing two reinforcing chiral catalysts has been developed. Continuous regeneration of the achiral starting material is effected via selective enzyme-catalyzed hydrolysis of the minor product enantiomer from Lewis acid-Lewis base catalyzed addition of acyl cyanides to prochiral aldehydes in a two-phase solvent system. The process provides O-acylated cyanohydrins in close to perfect enantioselectivities, higher than those obtained in the direct process, and in high yields. A combination of a (S,S)-salen Ti Lewis acid and Candida antarctica lipase B provides the products with R absolute configuration, whereas the opposite enantiomer is obtained from the (R,R)-salen Ti complex and Candida rugosa lipase." @default.
• W2024641109 created "2016-06-24" @default.
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• W2024641109 date "2009-11-09" @default.
• W2024641109 modified "2023-09-26" @default.
• W2024641109 title "Minor Enantiomer Recycling: Metal Catalyst, Organocatalyst and Biocatalyst Working in Concert" @default.
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• W2024641109 doi "https://doi.org/10.1002/chem.200901338" @default.
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