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- W2024663048 abstract "The construction and utilization of a column-shaped in situ thin-layer ESR spectroelectrochemical cell for both ambient and low temperature operation is reported. The working electrode is a columnshaped expanded platinum sheet of 9.4 × 4.0 mm that is placed in a 0.25 mm thick column-shaped, thin-layer chamber. The solution volume in the thin-layer chamber is 12 μL, and the total solution volume in the cell ranges between 1 and 3 mL. The application of this cell is demonstrated by time-resolved ESR spectra for electrooxidized porphyrins in methylene chloride solutions containing 0.3 M tetrabutylammonium perchlorate. The electrochemical behavior of this cell is also demonstrated by the oxidation of ferrocene under the same solution conditions at temperatures between 23 and −75°C. Well-defined ESR spectra are obtained in as short as 5–10 seconds without data manipulation." @default.
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- W2024663048 date "1990-01-01" @default.
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- W2024663048 title "The construction of a column-shaped, thin-layer ESR spectroelectrochemical cell for use at both ambient and low temperatures in nonaqueous solvents" @default.
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- W2024663048 doi "https://doi.org/10.1002/elan.1140020105" @default.
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