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- W2024752401 abstract "Electrochemical trifluoromethylation of 3-sulpholene (1) in a CF3COOH/CF3COONa/CH3CN/H2O system gives a complex mixture consisting of meso- and DL-3,4-bis(trifluorometayl)sulpholanes (2a) and (2b) as the major components and isomeric trifluoromethylsulpholenes 3a and 3b, 3,4-bis(trifluoromethyl)sulpholenes 4a and 4b, 3-trifluoromethylsulpholane 5 and 2,3,4-tris(trifluoromethyl) sulpholanes 6a-c as the minor components with a 40–50% total yield. Compounds 2a and 2b were efficiently isolated from the crude reaction mixture and fully identified by spectral methods. The reaction conducted in a CF3COOH/CF3COONa/H2O system, without acetonitrile, gave 4-trifluoromethyl-2-sulpholene (3a) as the main product, albeit total yield was low." @default.
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- W2024752401 date "1998-02-01" @default.
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- W2024752401 title "Electrochemical trifluoromethylation of 3-sulpholene. Synthesis of meso- and DL-3,4-bis(trifluoromethyl) sulpholanes" @default.
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- W2024752401 doi "https://doi.org/10.1016/s0022-1139(97)00142-5" @default.
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